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Beilstein J. Org. Chem. 2019, 15, 1129–1140, doi:10.3762/bjoc.15.109
Graphical Abstract
Figure 1: The ligands (i) L1 and (ii) L2 that are positional isomers (regioisomers).
Scheme 1: (i)/(ii) Complexation of Pd(tmeda)(Y)2 with the ligand L1 at 1:1 and 2:3 metal-to-ligand ratios, re...
Figure 2: Partial 1H NMR spectra in DMSO-d6 for (i) L1, (ii) [Pd(tmeda)(L1)](NO3)2 (1a) and (iii) a mixture o...
Figure 3: Partial 1H NMR spectra in DMSO-d6 for (i) L1, (ii) [Pd(L1)2](NO3)2 (3a) and (iii) [(NO3)2@Pd3(L1)4]...
Figure 4: Energy-minimized structures of (i) [Pd(tmeda)(L1)]2+, (ii) [Pd3(tmeda)3(L1)2]6+, (iii) [Pd(L1)2]2+,...
Scheme 2: Reorganization of (i) a mixture of Pd(NO3)2 and 3a at a 2:1 ratio leading to 4a with a complete con...
Scheme 3: Halide (F−, Cl− and Br− but not I−) encapsulation by the cavities of the double-decker cage.
Figure 5: Partial 1H NMR spectra at 400 MHz in DMSO-d6 for (i) [(NO3)2@Pd3(L1)4](NO3)4 (4a), (ii) [(F)2@Pd3(L1...